1,4-Dimethoxybenzene → 2,2,3,4,4,4-Hexafluorobutyl methacrylate
反応式
[C:1](Cl)(=[O:5])[C:2]([CH3:4])=[CH2:3].[F:7][C:8]([F:17])([CH:11]([F:16])[C:12]([F:15])([F:14])[F:13])[CH2:9][OH:10].COC1C=CC(OC)=CC=1>>[C:1]([O:10][CH2:9][C:8]([F:17])([F:7])[CH:11]([F:16])[C:12]([F:15])([F:13])[F:14])(=[O:5])[C:2]([CH3:4])=[CH2:3]参加物
4
実験手順
To 12 parts of methacrylic acid chloride were added 60 parts of 2,2,3,4,4,4-hexafluorobutyl alcohol as a reactant and a solvent and 0.1 part of hydroquinone dimethyl ether as a polymerization inhibitor. The mixture was heated at a temperature of 90° to 100° C. for 3 hours. The reaction mixture was distilled to give 15 parts of 2,2,3,4,4,4-hexafluorobutyl methacrylate (hereinafter referred to as "HFBMA") having a boiling point of 60° to 63° C./20 mmHg.
後処理
- temperatureThe mixture was heated at a temperature of 90° to 100° C. for 3 hours
- distillationThe reaction mixture was distilled
出典と根拠
- ORDレコード
- ord-50543bc6295b422e96997e76c434c439
- 出典データセット
- uspto-grants-1987_08
- 特許番号
- US04686168
反応ノート
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