1-Methylimidazole → 1-Hexadecyl-3-methylimidazolium Chloride

HRID 1819515ノート

反応式

HRID 1819515 の反応式
[Cl:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17].[CH3:18][N:19]1[CH:23]=[CH:22][N:21]=[CH:20]1>>[Cl-:1].[CH3:18][N+:19]1[CH:23]=[CH:22][N:21]([CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])[CH:20]=1

参加物

3

反応物 2

HCID 13901-MethylimidazoleHCID 209931-Chlorohexadecane

生成物 1

HCID 27342311-Hexadecyl-3-methylimidazolium Chloride

実験手順

The procedure of Example 1 was repeated with minor changes. 868 g of 1-chlorohexadecane and 570 g of 1-methylimidazole were added into a 2000 ml three-neck round-bottom flask. The reaction temperature was set from 95 to 100° C. After four hours the milk-like solution transferred into homogenous solution. The reaction was continued for three days. Then, the product was washed with ethyl acetate five times and toluene three times. After that, it was dried under vacuum for three days.

後処理

  1. customwas set from 95 to 100° C
  2. waitThe reaction was continued for three days
  3. washThen, the product was washed with ethyl acetate five times and toluene three times
  4. customAfter that, it was dried under vacuum for three days

出典と根拠

ORDレコード
ord-d9214cb717424488bbed2565859025e2
出典データセット
uspto-grants-2009_10
特許番号
US07601772B2

反応ノート

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