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8-Methoxy-3,4-dihydronaphthalen-1(2H)-one → 8-Methoxy-1,2,3,4-tetrahydronaphthalen-1-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 8-Methoxy-3,4-dihydronaphthalen-1(2H)-one | HCID 11275335 | — |
| 反応物 | 4,5,6,7-Tetrahydro-1-benzofuran-4-amine | HCID 18525171 | — |
| 生成物 | 8-Methoxy-1,2,3,4-tetrahydronaphthalen-1-amine | HCID 22147356 | — |
反応手順
Following the procedure for the preparation of 4,5,6,7-tetrahydro-1-benzofuran-4-amine but substituting 8-methoxy-3,4-dihydronaphthalen-1(2H)-one and making non-critical variations provided the title compound as a oil: 1H NMR (300 MHz, CDCl3) δ) 7.13, 6.73, 4.21, 3.87, 2.78–2.72, 1.88; HRMS (FAB) calcd for C11H15NO+H 178.1232, found 178.1232.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07041672B2 |
| 出典データセット | uspto-grants-2006_05 |
| ORD ID | ord-f51735332e5c4c0eb82df659798e23d3 |
| 出典メモ | uspto-grants-2006_05 |