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Acetone → Ethyl 6-methylnicotinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetone | HCID 180 | — |
| 反応物 | 1-(6-Methylpyridin-3-yl)butane-1,3-dione | HCID 20212814 | — |
| 生成物 | Ethyl 6-methylnicotinate | HCID 281994 | — |
反応手順
The 6-methylnicotinoyl-acetone which is mentioned as the starting substance in Example 6, can be obtained in a known manner from α-picoline-5-carboxylic acid ethyl ester and acetone, or from 5-acetyl-α-picoline (prepared in accordance with Angew. Ch. 67, page 398) and ethyl acetate:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04066768 |
| 出典データセット | uspto-grants-1978_01 |
| ORD ID | ord-7302fab9ec1b477bad43ebb018842f53 |
| 出典メモ | uspto-grants-1978_01 |