3-Nitrophenylethyl alcohol → 2-(3-Nitrophenyl)acetaldehyde
反応式
[N+:1]([C:4]1[CH:5]=[C:6]([CH2:10][CH2:11][OH:12])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].OI1(=O)C2C=CC=CC=2C(=O)O1>O1CCCC1>[N+:1]([C:4]1[CH:5]=[C:6]([CH2:10][CH:11]=[O:12])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2]参加物
4
実験手順
A mixture of 10 g of 2-(3-nitrophenyl)ethanol, 25.1 g of 1-hydroxy-1,2-benziodoxol-3(1H)-one 1-oxide and 300 ml of tetrahydrofuran is heated at reflux for 6 hours. After filtration and concentration of the solvent, the product is used as it is in the following Step.
後処理
- temperatureis heated
- temperatureat reflux for 6 hours
- filtrationAfter filtration and concentration of the solvent
出典と根拠
- ORDレコード
- ord-d3e402bd917e4f69915b77f47a8198ff
- 出典データセット
- uspto-grants-2004_08
- 特許番号
- US06784183B2
反応ノート
読み込み中…