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Uracil → Benzyl chloromethyl ether
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Uracil | HCID 1174 | — |
| 反応物 | Lumazine | HCID 10250 | — |
| 反応物 | 2-Chloromethyl 2-(trimethylsilyl)ethyl ether | HCID 2724271 | — |
| 生成物 | Benzyl chloromethyl ether | HCID 137983 | — |
反応手順
In a similar manner to the procedures described in Reference Example 3, reactions were carried out using pteridin-2,4-dione, instead of pyrimidine-2,4-dione, and using 2-(trimethylsilyl)ethoxymethyl chloride, instead of benzyloxymethyl chloride, to give the title compound (yield 53%) as a yellow powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06673804B1 |
| 出典データセット | uspto-grants-2004_01 |
| ORD ID | ord-85db933605be4fb6a518977183ca41e0 |
| 出典メモ | uspto-grants-2004_01 |