化工社化工社 化学情報印刷レポート · 研究参考用
Ammonium Oxalate → Palladium Platinum Tin Zirconium Oxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonium Oxalate | HCID 14213 | — |
| 反応物 | Tetraammineplatinum dinitrate | HCID 146543 | — |
| 反応物 | Zirconium oxide | HCID 6452892 | — |
| 反応物 | Oxalate;tin(4+) | HCID 9839089 | — |
| 反応物 | Palladium(II) nitrate hydrate | HCID 16211503 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Palladium Platinum Tin Zirconium Oxide | HCID 131732519 | — |
反応手順
The catalyst was synthesized using impregnation method. 10 g of the above crushed zirconium oxide (0.85 mm and 1.18 mm) was placed in a round bottom reactor. 0.56 g of tin oxalate and 0.54 g of ammonium oxalate was dissolved in 10 ml of water. 0.3 g of palladium nitrate hydrate, tetraammineplatinum(II) nitrate, was added to the tin oxalate solution, followed by impregnating to the above zirconium oxide by stepwise incipient wetness using a rotating dryer. The metal-coated zirconium oxide was dried and calcined under the conditions in Example 1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08962897B2 |
| 出典データセット | uspto-grants-2015_02 |
| ORD ID | ord-97b68a6f7bcd429eb98353f29b39a8b9 |
| 出典メモ | uspto-grants-2015_02 |