Propyl isocyanate → HCID 23348749、化合物

HRID 1855777

反応式

HRID 1855777 の反応式
[Cl:1][C:2]1[CH:14]=[CH:13][C:5]([CH2:6][NH:7][CH:8]2[CH2:12][CH2:11][CH2:10][CH2:9]2)=[CH:4][CH:3]=1.[CH2:15]([N:18]=[C:19]=[O:20])[CH2:16][CH3:17]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:6][N:7]([CH:8]2[CH2:12][CH2:11][CH2:10][CH2:9]2)[C:19]([NH:18][CH2:15][CH2:16][CH3:17])=[O:20])=[CH:13][CH:14]=1

参加物

3

反応物 2

HCID 61033Propyl isocyanateHCID 8340834-chloro-N-cyclopentylbenzylamine

生成物 1

HCID 23348749HCID 23348749、化合物収率 73.4%

実験手順

In a manner analogous to that described in Example 1, 31 g of N-4-chlorobenzyl-N-cyclopentylamine were reacted with 13 g of propyl isocyanate. 32 g of N-4-chlorobenzyl-N-cyclopentyl-N'-propylurea were obtained. Melting point: 103°-105° C.

出典と根拠

ORDレコード
ord-dde939c73ee648248c00ae8dad8d0b21
出典データセット
uspto-grants-1980_08
特許番号
US04216228

関連ノート

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