化工社化工社 化学情報印刷レポート · 研究参考用
Methyl behenate → (2-Morpholinoethyl) behenate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl behenate | HCID 13584 | — |
| 反応物 | 2-Morpholinoethanol | HCID 61163 | — |
| 触媒 | Sodium Methoxide | HCID 10942334 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | (2-Morpholinoethyl) behenate | HCID 66705417 | 91% |
反応手順
A mixture of 35.5 g of methyl behenate (18), 19.7 g of 2-morpholinoethanol (17), 270 mg of sodium methoxide and 150 g of toluene was heated under reflux for 6 hours while distilling off the methanol resulting from the reaction. The reaction solution was cooled. By standard aqueous work-up and distilling off toluene, 41.3 g of (2-morpholinoethyl) behenate (Quencher 2) was obtained (yield 91%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07629108B2 |
| 出典データセット | uspto-grants-2009_12 |
| ORD ID | ord-a386f213e6bd46459c2ea17f0bb9ba1b |
| 出典メモ | uspto-grants-2009_12 |