Methylamine → HCID 69077690、化合物
反応式
[F:1][C:2]([F:19])([F:18])[C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][N:11]2[C:15](=[O:16])[CH2:14][O:13][C:12]2=[O:17])=[CH:5][CH:4]=1.[CH3:20][NH2:21]>CO.O1CCCC1>[F:1][C:2]([F:19])([F:18])[C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][NH:11][C:12](=[O:17])[O:13][CH2:14][C:15]([NH:21][CH3:20])=[O:16])=[CH:5][CH:4]=1参加物
5
実験手順
A solution of 0.75 g (2.74 mmol) of 3-{2-[4-(trifluoromethyl)phenyl]ethyl}-1,3-oxazolidine-2,4-dione obtained in step 2.1., in 10 ml of methanol is admixed with 8 ml (16.47 mmol) of a solution (2M) of methylamine in tetrahydrofuran. Stirring is continued at ambient temperature for 12 hours.
出典と根拠
- ORDレコード
- ord-8c15987a174f4330bf03349a6190d56c
- 出典データセット
- uspto-grants-2009_12
- 特許番号
- US07632850B2
反応ノート
読み込み中…