Isobutyraldehyde → 1,1-Dimethylethyl 2-(2-methylpropylidene)hydrazinecarboxylate

反応式

[CH:1](=O)[CH:2]([CH3:4])[CH3:3].[C:6]([O:10][C:11](=[O:14])[NH:12][NH2:13])([CH3:9])([CH3:8])[CH3:7]>>[C:6]([O:10][C:11]([NH:12][N:13]=[CH:1][CH:2]([CH3:4])[CH3:3])=[O:14])([CH3:9])([CH3:8])[CH3:7]

参加物

反応物 2

HCID 6561Isobutyraldehyde

HCID 70091tert-Butyl carbazate

生成物 1

HCID 852555401,1-Dimethylethyl 2-(2-methylpropylidene)hydrazinecarboxylate

実験手順

B-21a is prepared analogously to B-19a starting from isobutyraldehyde (1.26 mL, 13.9 mmol) and tert-butylcarbazate (1.83 g, 13.9 mmol). Yield: 2.56 g.

後処理

customB-21a is prepared analogously to B-19a

出典と根拠

ORDレコード: ord-ba3fd5808a4c483da23791ef3b674f87
出典データセット: uspto-grants-2012_11
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08304556B2

反応ノート

読み込み中…