Thionyl Chloride → HCID 68515497、化合物

HRID 1877062ノート

反応式

HRID 1877062 の反応式
[CH3:1][CH:2]([CH3:18])[CH2:3][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])O.S(Cl)([Cl:21])=O>C1(C)C=CC=CC=1>[Cl:21][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])[CH2:3][CH:2]([CH3:18])[CH3:1]

参加物

4

反応物 2

HCID 24386Thionyl ChlorideHCID 685095783-Methyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol

生成物 1

HCID 68515497HCID 68515497、化合物収率 100%

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

To a solution of 3-methyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol (1.5 g) in toluene (20 mL) was added thionyl chloride (0.9 mL), and the mixture was stirred at room temperature overnight. The solvent was evaporated under reduced pressure to give the title compound (1.6 g, 100%) as an oil.

後処理

  1. customThe solvent was evaporated under reduced pressure

出典と根拠

ORDレコード
ord-059cce386ae5449980b3c2710eff9d05
出典データセット
uspto-grants-2012_11
特許番号
US08309580B2

反応ノート

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