Ammonia → Ammonium nitrate

HRID 1879520ノート

反応式

HRID 1879520 の反応式
[NH2:1][NH2:2].[N+:3]([O-:6])([O-:5])=[O:4].[NH4+].N>>[N+:3]([O-:6])([OH:5])=[O:4].[NH2:1][NH2:2].[N+:3]([O-:6])([O-:5])=[O:4].[NH4+:3]

参加物

5

実験手順

Hydrazine nitrate (HN) was prepared by reacting anhydrous hydrazine with an equivalent amount of ammonium nitrate. Formation took place by displacement of the ammonia as a gas. In production the ammonia would be scavenged by passing it through an aqueous nitric acid solution trap to form ammonium nitrate, which could then be used to prepare more HN. The HN product was purified by crystallization from methanol. This process was quite safe because it eliminated the need to neutralize the hydrazine with nitric acid. The procedure used is as follows.

出典と根拠

ORDレコード
ord-3eb90de0e70a4b148fb2c4f0587e0fd1
出典データセット
uspto-grants-2012_11
特許番号
US08317952B2

反応ノート

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