ホームMCPワークベンチSkills
ホームワークベンチ通知マイページ
llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
  1. ホーム
  2. /反応

Water → 5-Bromo-1,3-dichloro-2-(difluoromethoxy)benzene

HRID 1880259
ノート
印刷プレビュー

反応式

HRID 1880259 の反応式
[Br:1][C:2]1[CH:7]=[C:6]([Cl:8])[C:5]([OH:9])=[C:4]([Cl:10])[CH:3]=1.C(=O)([O-])[O-].[K+].[K+].Br[C:18]([F:25])([F:24])C(OCC)=O.O>C(#N)C>[Br:1][C:2]1[CH:7]=[C:6]([Cl:8])[C:5]([O:9][CH:18]([F:25])[F:24])=[C:4]([Cl:10])[CH:3]=1
参加物実験手順後処理出典と根拠反応ノート

参加物

6

反応物 4

HCID 962WaterHCID 11430Potassium CarbonateHCID 185874-Bromo-2,6-dichlorophenolHCID 69585Ethyl bromodifluoroacetate

生成物 1

HCID 668657425-Bromo-1,3-dichloro-2-(difluoromethoxy)benzene

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

To a solution of 2.3 g of 4-bromo-2,6-dichlorophenol in 25 mL of acetonitrile, 1.3 g of potassium carbonate and 3.8 g of ethyl bromodifluoroacetate were added and the resultant mixture was stirred while heating the mixture to reflux for 4 hours. After the completion of the reaction, the reaction mixture was left to be cooled down to room temperature and charged into 100 mL of water and the resultant mixture was extracted with ethyl acetate (100 mL×1). The organic phase was washed with water and then dehydrated and dried over saturated saline and anhydrous sodium sulfate in this order and the solvent was distilled off under reduced pressure. The resultant residue was purified by silica gel column chromatography eluting with ethyl acetate-hexane (1:4) to obtain 2.4 g of the objective substance as a yellow oily substance.

後処理

  1. temperaturewhile heating the mixture
  2. temperatureto reflux for 4 hours
  3. customAfter the completion of the reaction
  4. waitthe reaction mixture was left
  5. extractionthe resultant mixture was extracted with ethyl acetate (100 mL×1)
  6. washThe organic phase was washed with water
  7. dry with materialdried over saturated saline and anhydrous sodium sulfate in this order
  8. distillationthe solvent was distilled off under reduced pressure
  9. customThe resultant residue was purified by silica gel column chromatography
  10. washeluting with ethyl acetate-hexane (1:4)
  11. customto obtain 2.4 g of the objective substance as a yellow oily substance

出典と根拠

ORDレコード
ord-5d402632bb754b91a7fd1c6bc7b238ba
出典データセット
uspto-grants-2012_11
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US08318757B2

反応ノート

読み込み中…

このページの内容参加物実験手順後処理出典と根拠反応ノート