Silver Nitrate → Acesulfame silver

HRID 1883215

反応式

HRID 1883215 の反応式
[N+]([O-])([O-])=O.[Ag+:5].[CH3:6][C:7]1[O:15][S:12](=[O:14])(=[O:13])[N-:11][C:9](=[O:10])[CH:8]=1.[K+]>O>[CH3:6][C:7]1[O:15][S:12](=[O:14])(=[O:13])[NH:11][C:9](=[O:10])[CH:8]=1.[Ag:5]

参加物

4

反応物 2

HCID 24470Silver NitrateHCID 11074431Acesulfame Potassium

生成物 1

HCID 131724477Acesulfame silver収率 88%

試薬・触媒・溶媒 1

HCID 962Water溶媒2 回

実験手順

A solution of 30 mmol (5.148 g) of silver(I) nitrate in 30 ml of water was added to a solution of 30 mmol (6.037 g) of acesulfame-K in 30 ml of water. After addition was complete, the colorless precipitate formed was filtered off by suction and washed twice, each time with 10 ml of water. 88% of colorless acesulfame-silver crystals resulted. The reaction and subsequent workup as described above need not be carried out in the absence of light.

後処理

  1. additionAfter addition
  2. customthe colorless precipitate formed
  3. filtrationwas filtered off by suction
  4. washwashed twice

出典と根拠

ORDレコード
ord-a719c7edd0914d6fa57be7d45727584e
出典データセット
uspto-grants-2004_07
特許番号
US06759544B2

関連ノート

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