HCID 69859806、化合物 → HCID 23508311、化合物
反応式
[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([C:14]([CH3:21])=[CH:15][C:16]([O:18][CH2:19][CH3:20])=[O:17])=[C:9]2[C:13]=1[CH2:12][CH2:11][CH2:10]2)(=[O:3])[CH3:2]>C(O)C.[Pd]>[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([CH:14]([CH3:21])[CH2:15][C:16]([O:18][CH2:19][CH3:20])=[O:17])=[C:9]2[C:13]=1[CH2:12][CH2:11][CH2:10]2)(=[O:3])[CH3:2]参加物
4
実験手順
A solution of ethyl 3-[7-acetylamino-indan-4-yl]-but-2-enoate (1.9 g, Reference Example 7) in ethanol (200 mL) was hydrogenated over 10% palladium on charcoal for 16 hours. The mixture was filtered through diatomaceous earth and the filtrate was evaporated to give the title compound (1.66 g).
後処理
- filtrationThe mixture was filtered through diatomaceous earth
- customthe filtrate was evaporated
出典と根拠
- ORDレコード
- ord-434ee3510dec4a728e8def25a85bbf26
- 出典データセット
- uspto-grants-2004_07
- 特許番号
- US06762199B2
反応ノート
読み込み中…