Thionyl Chloride → Chloromethyl chloroisopropyl benzene
反応式
S(Cl)([Cl:3])=O.[Cl:5][C:6]1[C:13]([CH:14]([CH3:16])[CH3:15])=[CH:12][CH:11]=[CH:10][C:7]=1[CH2:8]O>C(Cl)(Cl)(Cl)Cl>[Cl:5][C:6]1[C:13]([CH:14]([CH3:16])[CH3:15])=[CH:12][CH:11]=[CH:10][C:7]=1[CH2:8][Cl:3]参加物
4
反応条件
- 温度
- 25 °C
実験手順
At room temperature, 29.8 g of thionyl chloride is carefully dripped into 35 g of 2-chloro-3-isopropylbenzyl alcohol in 80 ml of carbon tetrachloride. The mixture is stirred for 15 hours at 25° C. and then evaporated down. Distillation (bp 0.3 :76°-78° C.) gives 33 g of 2-chloro-3-isopropylbenzyl chloride.
後処理
- customAt room temperature
- customevaporated down
- distillationDistillation (bp 0.3 :76°-78° C.)
出典と根拠
- ORDレコード
- ord-fc3b6c140b8a4c1da8960675eeae99fb
- 出典データセット
- uspto-grants-1992_09
- 特許番号
- US05147645
反応ノート
読み込み中…