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Methanol → Methyl 4-bromocinnamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | p-Bromocinnamic acid | HCID 99777 | — |
| 生成物 | Methyl 4-bromocinnamate | HCID 816774 | — |
反応手順
To a stirred solution of 4-bromocinnamic acid (16 g) in methanol (150 mL) was added thionyl chloride (30 mL) at 0° C. The reaction mixture was warmed to room temperature and refluxed for 3 hours. After cooling to room temperature the solvents were evaporated to dryness. The crude compound obtained was used as such for the next step.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08507670B2 |
| 出典データセット | uspto-grants-2013_08 |
| ORD ID | ord-1453db34cac84fa79f365c1ae16913b0 |
| 出典メモ | uspto-grants-2013_08 |