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Dimethylformamide → 5-Methoxyacetylamino-2,4,6-triiodoisophthalic acid (2,3-dihydroxypropyl)amide chloride

HRID 1902605
ノート
印刷プレビュー

反応式

HRID 1902605 の反応式
[CH3:1][O:2][CH2:3][C:4]([NH:6][C:7]1[C:8]([I:21])=[C:9]([C:18](Cl)=[O:19])[C:10]([I:17])=[C:11]([C:15]=1[I:16])[C:12]([Cl:14])=[O:13])=[O:5].C(N(CCCC)CCCC)CCC.[OH:35][CH:36]([CH2:39][OH:40])[CH2:37][NH2:38].CN(C=[O:45])C>>[Cl-:14].[OH:35][CH:36]([CH2:39][OH:40])[CH2:37][NH:38][C:18](=[O:19])[C:9]1[C:8]([I:21])=[C:7]([NH:6][C:4](=[O:5])[CH2:3][O:2][CH3:1])[C:15]([I:16])=[C:11]([C:12]([OH:45])=[O:13])[C:10]=1[I:17]
参加物反応条件実験手順後処理出典と根拠反応ノート

参加物

5

反応物 4

HCID 6228Dimethylformamide2 回HCID 7622TributylamineHCID 735613-Amino-1,2-propanediolHCID 135899615-Methoxyacetamido-2,4,6-triiodoisophthaloyl chloride

生成物 1

HCID 866509085-Methoxyacetylamino-2,4,6-triiodoisophthalic acid (2,3-dihydroxypropyl)amide chloride

反応条件

温度
60 °C

実験手順

50 g. (75 mmol) of 5-methoxyacetylamino-2,4,6-triiodoisophthalic acid dichloride is dissolved in 200 ml. of dry DMF; 18 g. (97.3 mmol) of tributylamine is added thereto, the mixture is heated to 60° C., and, at this temperature, a solution of 7.5 g. (82.4 mmol) of 2,3-dihydroxypropylamine in 50 ml. of DMF is added dropwise thereto. The mixture is stirred for 2 hours at 60° C., then concentrated to 100 ml., and stirred into 1.2 l. of methylene chloride. The precipitate thus formed is vacuum-filtered, dried, refluxed twice with respectively 500 ml. of ethyl acetate, and filtered in the hot state. The evaporated filtrate yields 40.5 g. (56 mmol)=74.5% of theory of the desired product as a colorless solid.

後処理

  1. concentrationconcentrated to 100 ml
  2. stirring, and stirred into 1.2 l
  3. customThe precipitate thus formed
  4. filtrationis vacuum-filtered
  5. customdried
  6. temperaturerefluxed twice with respectively 500 ml
  7. filtrationof ethyl acetate, and filtered in the hot state
  8. customThe evaporated filtrate yields 40.5 g

出典と根拠

ORDレコード
ord-875430f714694d3185cad83fec7dfa28
出典データセット
uspto-grants-1982_12
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04364921

反応ノート

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