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Hexyl carbamate → Dihexyl carbonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hexyl carbamate | HCID 75026 | — |
| 触媒 | zinc II acetate | HCID 131713426 | — |
| 生成物 | Dihexyl carbonate | HCID 522576 | 93.9% |
反応手順
The procedure described in Example 11 is followed, but additionally 0.5 part of zinc-II acetate is included in the reaction mixture. Analysis by gas chromatography shows that within the same period of time 94% of the n-hexyl carbamate are converted and 20.3 parts of di-n-hexyl carbonate (93.9% of theory, based on converted n-hexyl carbamate), of boiling point 122°-124° C./4 mbar have been formed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04436668 |
| 出典データセット | uspto-grants-1984_03 |
| ORD ID | ord-e48fef429dfc4481bdcb19bba357884e |
| 出典メモ | uspto-grants-1984_03 |