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3-(3-Phenyl-1-propenyl)aniline → 3-(3-Phenylpropyl)aniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(3-Phenyl-1-propenyl)aniline | HCID 54042989 | — |
| 触媒 | HCID 178418390 | HCID 178418390 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 3-(3-Phenylpropyl)aniline | HCID 427307 | 92% |
反応手順
A solution of 3-(3-phenyl-1-propenyl)aniline (3.6 g) in 50 ml of ethanol was subjected to catalytic reduction using 1 g of 10% palladium-carbon. After removal of the catalyst by filtration, the solvent was removed under reduced pressure. The residue was distilled under reduced pressure to give 3.3 g of 3-(3-phenylpropyl)aniline (yield, 92%). B.P. 122°-126° C./0.08 mmHg.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04437880 |
| 出典データセット | uspto-grants-1984_03 |
| ORD ID | ord-14973120f72e4eb5953e84b360c0baf4 |
| 出典メモ | uspto-grants-1984_03 |