HRID1903652

反应详情

EQUATION

反应方程式

HRID 1903652 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 3-(3-phenyl-1-propenyl)aniline (3.6 g) in 50 ml of ethanol was subjected to catalytic reduction using 1 g of 10% palladium-carbon. After removal of the catalyst by filtration, the solvent was removed under reduced pressure. The residue was distilled under reduced pressure to give 3.3 g of 3-(3-phenylpropyl)aniline (yield, 92%). B.P. 122°-126° C./0.08 mmHg.

WORKUP

后处理

  1. customAfter removal of the catalyst
  2. filtrationby filtration
  3. customthe solvent was removed under reduced pressure
  4. distillationThe residue was distilled under reduced pressure