Ammonia → Ammonium nitrate

HRID 1915980ノート

反応式

HRID 1915980 の反応式
[NH2:1][NH2:2].[N+:3]([O-:6])([O-:5])=[O:4].[NH4+].N>>[N+:3]([O-:6])([OH:5])=[O:4].[NH2:1][NH2:2].[N+:3]([O-:6])([O-:5])=[O:4].[NH4+:3]

参加物

5

実験手順

Hydrazine nitrate (HN) was prepared by reacting anhydrous hydrazine with an equivalent amount of ammonium nitrate. Formation took place by displacement of the ammonia as a gas. In production the ammonia would be scavenged by passing it through an aqueous nitric acid solution trap to form ammonium nitrate, which could then be used to prepare more HN. The HN product was purified by crystallization from methanol. This process was quite safe because it eliminated the need to neutralize the hydrazine with nitric acid. The procedure used is as follows.

出典と根拠

ORDレコード
ord-0d64f0441d1f4304b9ffb109bf28693e
出典データセット
uspto-grants-2013_12
特許番号
US08617327B1

反応ノート

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