Hydrochloric Acid → Sodium 1,1,3,3,3-pentafluoro-2-hydroxypropane-1-sulfonate
反応式
[F:1][C:2]([F:19])([S:15]([O-:18])(=[O:17])=[O:16])[CH:3]([O:8]C(=O)C(C)(C)C)[C:4]([F:7])([F:6])[F:5].[Na+:20].[OH-].[Na+].Cl>CO>[F:19][C:2]([F:1])([S:15]([O-:18])(=[O:16])=[O:17])[CH:3]([OH:8])[C:4]([F:5])([F:7])[F:6].[Na+:20]参加物
5
実験手順
Ester hydrolysis reaction was effected using sodium 1,1,3,3,3-pentafluoro-2-(pivaloyloxy)propanesulfonate, which was prepared according to the formulation described in JP-A 2007-145797, and a sodium hydroxide aqueous solution in methanol. After the completion of reaction, hydrochloric acid was added to turn the reaction system from neutral to weakly acidic. The aqueous solution was directly used in the subsequent reaction.
後処理
- customwas prepared
- additionwas added
- customThe aqueous solution was directly used in the subsequent reaction
出典と根拠
- ORDレコード
- ord-116a2f7ce61747d4b102643fe2f87669
- 出典データセット
- uspto-grants-2012_05
- 特許番号
- US08173354B2
反応ノート
読み込み中…