Hydrazine hydrate (1:1) → 4-iodo-5-methyl-1H-pyrazolo[3,4-b]pyridine
反応式
F[C:2]1[C:7]([CH:8]=O)=[C:6]([I:10])[C:5]([CH3:11])=[CH:4][N:3]=1.O.[NH2:13][NH2:14]>O1CCOCC1>[I:10][C:6]1[C:5]([CH3:11])=[CH:4][N:3]=[C:2]2[NH:13][N:14]=[CH:8][C:7]=12参加物
4
実験手順
2-fluoro-4-iodo-5-methyl-pyridine-3-carbaldehyde (510 mg, 1.924 mmol) was dissolved in dry Dioxane (10 mL) and Hydrazine monohydrate (288.9 mg, 280.8 μL, 5.772 mmol) was added in one portion
出典と根拠
- ORDレコード
- ord-0e3dba08173946638dd3ddb772ce9631
- 出典データセット
- uspto-grants-2012_05
- 特許番号
- US08173635B2
反応ノート
読み込み中…