Methyl triflate → 3-(cyclopropyl-methyl-sulfamoyl)-1-methyl-3-H-imidazol-1-ium trifluoromethanesulfonate
反応式
[CH:1]1([N:4]([CH3:13])[S:5]([N:8]2[CH:12]=[CH:11][N:10]=[CH:9]2)(=[O:7])=[O:6])[CH2:3][CH2:2]1.[O:14](C)[S:15]([C:18]([F:21])([F:20])[F:19])(=[O:17])=[O:16]>>[F:19][C:18]([F:21])([F:20])[S:15]([O-:17])(=[O:16])=[O:14].[CH:1]1([N:4]([CH3:13])[S:5]([N:8]2[CH:12]=[CH:11][N+:10]([CH3:18])=[CH:9]2)(=[O:6])=[O:7])[CH2:3][CH2:2]1参加物
3
実験手順
3-(Cyclopropyl-methyl-sulfamoyl)-1-methyl-3-H-imidazol-1-ium trifluoromethane-sulfonate was prepared in accordance with step B of the general method described in example 76 from imidazole-1-sulfonic acid cyclopropyl-methyl-amide and methyl triflate; MS: m/e=216.4 (M+).
出典と根拠
- ORDレコード
- ord-a4eb7202de4f47beaff9be99d45c9888
- 出典データセット
- uspto-grants-2012_05
- 特許番号
- US08183380B2
反応ノート
読み込み中…