Methyl triflate → 3-(Cyclopropylmethyl-methyl-sulfamoyl)-1-methyl-3-H-imidazol-1-ium trifluoromethanesulfonate
反応式
[CH:1]1([CH2:4][N:5]([CH3:14])[S:6]([N:9]2[CH:13]=[CH:12][N:11]=[CH:10]2)(=[O:8])=[O:7])[CH2:3][CH2:2]1.[O:15](C)[S:16]([C:19]([F:22])([F:21])[F:20])(=[O:18])=[O:17]>>[F:20][C:19]([F:22])([F:21])[S:16]([O-:18])(=[O:17])=[O:15].[CH:1]1([CH2:4][N:5]([CH3:14])[S:6]([N:9]2[CH:13]=[CH:12][N+:11]([CH3:19])=[CH:10]2)(=[O:8])=[O:7])[CH2:2][CH2:3]1参加物
3
実験手順
3-(Cyclopropylmethyl-methyl-sulfamoyl)-1-methyl-3-H-imidazol-1-ium trifluoromethanesulfonate was prepared in accordance with step B of the general method described in example 76 from imidazole-1-sulfonic acid cyclopropylmethyl-methyl-amide and methyl triflate; MS: m/e=230.4 (M−).
出典と根拠
- ORDレコード
- ord-f1af083f659c47a59c3eb7f47d76ab42
- 出典データセット
- uspto-grants-2012_05
- 特許番号
- US08183380B2
反応ノート
読み込み中…