alpha,beta-Diphenyl acrylic acid → 2,3-Diphenylpropionic acid
反応式
[C:1]1([C:7](=[CH:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:8]([OH:10])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1>[Pd].C(O)C>[C:1]1([CH:7]([CH2:11][C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:8]([OH:10])=[O:9])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1参加物
4
実験手順
10% Palladium on charcoal (0.8 g) was added to a solution of α-phenylcinnamic acid (10.0 g, 0.0445 mol) in ethanol (200 ml). The mixture was hydrogenated at ambient temperature. The mixture was filtered through Celite, and the solvent was evaporated.
後処理
- customwas hydrogenated at ambient temperature
- filtrationThe mixture was filtered through Celite
- customthe solvent was evaporated
出典と根拠
- ORDレコード
- ord-33cead44eac44e468313dedb95cecb85
- 出典データセット
- uspto-grants-2002_05
- 特許番号
- US06388090B2
反応ノート
読み込み中…