N-benzyl-6-(4-phenylbutoxy)hexan-1-amine → 6-(4-Phenylbutoxy)hexan-1-amine
反応式
C([NH:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][O:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)C1C=CC=CC=1>CCO.[Pd]>[C:20]1([CH2:19][CH2:18][CH2:17][CH2:16][O:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][NH2:8])[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1参加物
4
実験手順
A solution of 4.02 g (11.86 mmol) N-benzyl-6-(4-phenylbutoxy)hexylamine in 40 ml EtOH is hydrogenated at room temperature and atmospheric pressure with 0.4 g 5% Pd/C. When 300 ml H2 have been absorbed, the mixture is filtered on decalite and the filtrate is concentrated to yield 2.89 g (97.9%) 6-(4-phenylbutoxy)hexylamine as an oil.
後処理
- customis hydrogenated at room temperature
- customWhen 300 ml H2 have been absorbed
- filtrationthe mixture is filtered on decalite
- concentrationthe filtrate is concentrated
出典と根拠
- ORDレコード
- ord-f81998c366584b50bb1ceae388beb513
- 出典データセット
- uspto-grants-2002_05
- 特許番号
- US06388134B1
反応ノート
読み込み中…