Triethylamine → HCID 22462389、化合物
反応式
[CH2:1]([O:4][C:5]1[CH:13]=[CH:12][CH:11]=[CH:10][C:6]=1[C:7](Cl)=[O:8])[CH2:2][CH3:3].[NH2:14][C:15]1[C:16]([C:21]([NH2:23])=[O:22])=[N:17][CH:18]=[CH:19][CH:20]=1.C(N(CC)CC)C>C(#N)C>[CH2:1]([O:4][C:5]1[CH:13]=[CH:12][CH:11]=[CH:10][C:6]=1[C:7]([NH:14][C:15]1[C:16]([C:21]([NH2:23])=[O:22])=[N:17][CH:18]=[CH:19][CH:20]=1)=[O:8])[CH2:2][CH3:3]参加物
5
実験手順
In a similar manner to Example 68 a) reaction of 2-propoxybenzoyl chloride (0.99 g), 3-aminopicolinamide (0.69 g) and triethylamine (0.51 g) in acetonitrile (15 ml) afforded a crude product which was recrystallized from methanol to afford 3-(2-propoxybenzamido)picolinamide, 0.91 g, m.p. 116-118° C.
後処理
- customafforded a crude product which
- customwas recrystallized from methanol
出典と根拠
- ORDレコード
- ord-98d468e099334385a3dde73cc81e828a
- 出典データセット
- uspto-grants-2002_05
- 特許番号
- US06391885B1
反応ノート
読み込み中…