3-(4-ethylphenyl)prop-2-enoic Acid → 3-(4-ethylphenyl)propanoic Acid
反応式
[CH2:1]([C:3]1[CH:13]=[CH:12][C:6]([CH:7]=[CH:8][C:9]([OH:11])=[O:10])=[CH:5][CH:4]=1)[CH3:2]>[Pd].C(O)C>[CH2:1]([C:3]1[CH:13]=[CH:12][C:6]([CH2:7][CH2:8][C:9]([OH:11])=[O:10])=[CH:5][CH:4]=1)[CH3:2]参加物
4
実験手順
An ethanol (250 ml) solution of 4-ethyl cinnamic acid (34.0 g, 0.191 mol) was hydrogenated at 60 psi over 10% Pd/C (2 g) for 2 hr. The mixture was filtered and concentrated in vacuo to give 3-(4-ethylphenyl)propionic acid as a white solid (34 g, 100%).
後処理
- filtrationThe mixture was filtered
- concentrationconcentrated in vacuo
出典と根拠
- ORDレコード
- ord-0fc75f6f6b22454c91e58d00b6e81438
- 出典データセット
- uspto-grants-1998_07
- 特許番号
- US05780470
反応ノート
読み込み中…