3-(4-ethylphenyl)prop-2-enoic Acid → 3-(4-ethylphenyl)propanoic Acid
反応式
[CH2:1]([C:3]1[CH:13]=[CH:12][C:6]([CH:7]=[CH:8][C:9]([OH:11])=[O:10])=[CH:5][CH:4]=1)[CH3:2]>C(O)(=O)C.[Pd]>[CH2:1]([C:3]1[CH:13]=[CH:12][C:6]([CH2:7][CH2:8][C:9]([OH:11])=[O:10])=[CH:5][CH:4]=1)[CH3:2]参加物
4
実験手順
A solution containing 18 g of 4-ethylcinnamic acid dissolved in 50 mL of acetic acid was placed in a Parr Shaker bomb flask, 1.0 g of 5% palladium on carbon catalyst was added, and the flask was pressured to 50 psig (pounds per square inch gauge) (4460 kiloPascals) for 2 hours. The catalyst was then removed by filtration and the solution was concentrated by evaporation under reduced pressure. Water was added to the residue and the solid present was collected by filtration and dried under reduced pressure to obtain 3-(4-ethylphenyl)propanoic acid.
後処理
- additionwas added
- customThe catalyst was then removed by filtration
- concentrationthe solution was concentrated by evaporation under reduced pressure
- additionWater was added to the residue
- filtrationthe solid present was collected by filtration
- customdried under reduced pressure
出典と根拠
- ORDレコード
- ord-ca95abd84ef341a7997ba843f063a757
- 出典データセット
- uspto-grants-1998_07
- 特許番号
- US05780465
反応ノート
読み込み中…