Ethyl Bromide → 5-bromo-N-ethyl-2-methylaniline

反応式

Br[CH2:2][CH3:3].[Br:4][C:5]1[CH:6]=[CH:7][C:8]([CH3:12])=[C:9]([CH:11]=1)[NH2:10]>>[Br:4][C:5]1[CH:6]=[CH:7][C:8]([CH3:12])=[C:9]([CH:11]=1)[NH:10][CH2:2][CH3:3]

参加物

反応物 2

HCID 6332Ethyl Bromide

HCID 27348055-Bromo-o-toluidine

生成物 1

HCID 437296995-bromo-N-ethyl-2-methylaniline収率 71%

実験手順

Using the same method as in Example 22-(i), bromoethane was reacted with the 5-bromo-2-methylaniline to give 5-bromo-N-ethyl-2-methylaniline (yield: 71%).

出典と根拠

ORDレコード: ord-ea85080ab9de409f82c76c06ede6d6dc
出典データセット: uspto-grants-2013_04
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08415479B2

反応ノート

読み込み中…