3-Nitro-N-(pyridin-4-yl)pyridin-2-amine → HCID 12445535、化合物

HRID 1974324ノート

反応式

HRID 1974324 の反応式
[N+:1]([C:4]1[C:5]([NH:10][C:11]2[CH:16]=[CH:15][N:14]=[CH:13][CH:12]=2)=[N:6][CH:7]=[CH:8][CH:9]=1)([O-])=O>[Pd].CO>[NH2:1][C:4]1[C:5]([NH:10][C:11]2[CH:16]=[CH:15][N:14]=[CH:13][CH:12]=2)=[N:6][CH:7]=[CH:8][CH:9]=1

参加物

4

反応物 1

HCID 124453923-Nitro-N-(pyridin-4-yl)pyridin-2-amine

生成物 1

HCID 12445535HCID 12445535、化合物

試薬・触媒・溶媒 2

HCID 23938Palladium触媒HCID 887Methanol溶媒

実験手順

The nitro compound from Step A (1.0 g.) was hydrogenated in 60 ml. of methanol over 0.2 g. of 5% palladium on carbon catalyst. The catalyst was removed by filtration and the filtrate was evaporated to dryness.

後処理

  1. customThe catalyst was removed by filtration
  2. customthe filtrate was evaporated to dryness

出典と根拠

ORDレコード
ord-ea124cf1a6c54326bf7e664de0c6bc0c
出典データセット
uspto-grants-1976_12
特許番号
US04000286

反応ノート

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