Thionyl Chloride → HCID 23149173、化合物
反応式
[CH3:1][C:2]([C:6]1[N:10]=[CH:9][N:8]([CH2:11]O)[N:7]=1)([CH3:5])[CH2:3][CH3:4].S(Cl)([Cl:15])=O>ClCCl>[ClH:15].[Cl:15][CH2:11][N:8]1[CH:9]=[N:10][C:6]([C:2]([CH3:5])([CH3:1])[CH2:3][CH3:4])=[N:7]1参加物
4
実験手順
1.10 g of 3-(1,1-dimethylpropyl)-1H-1,2,4-triazole1-ylmethanol was dissolved to 18 ml of dichloromethane. 1.8 ml of thionyl chloride was added to the solution, followed by stirring at room temperature for 8 hours. The reaction mixture was concentrated under reduced pressure to obtain 1.47 g of 1-(chloromethyl)-3-(1,1-dimethylpropyl)-1H-1,2,4-triazole hydrochloride.
後処理
- concentrationThe reaction mixture was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-874d6d80cdbd411ea9933f36812f8cb7
- 出典データセット
- uspto-grants-2009_06
- 特許番号
- US07541374B2
反応ノート
読み込み中…