Methanol → Methyl 4-(methylamino)butanoate
反応式
Cl.[CH3:2][NH:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=[O:8].S(Cl)(Cl)=O.[CH3:14]O>>[CH3:14][O:8][C:7](=[O:9])[CH2:6][CH2:5][CH2:4][NH:3][CH3:2]参加物
4
反応条件
- 温度
- 0 °C
実験手順
4-(methylamino) butyric acid HCl was dissolved in methanol and thionyl chloride in catalytic amount was added drop by drop. The reaction mixture was stirred at 0° C. for 30 min. Thereafter, the solvent was reduced in vacu, yielding a white solid.
後処理
- customyielding a white solid
出典と根拠
- ORDレコード
- ord-a3dd38a54c534097bca325db7a81d19e
- 出典データセット
- uspto-grants-2010_01
- 特許番号
- US07645903B2
反応ノート
読み込み中…