Borane;tetrahydrofuran → HCID 23155228、化合物
反応式
[NH2:1][C:2]1[CH:3]=[C:4]([CH:10]=[C:11]([C:13]([F:16])([F:15])[F:14])[CH:12]=1)[C:5]([N:7]([CH3:9])[CH3:8])=O.B.C1COCC1>C1COCC1>[CH3:9][N:7]([CH2:5][C:4]1[CH:3]=[C:2]([NH2:1])[CH:12]=[C:11]([C:13]([F:16])([F:14])[F:15])[CH:10]=1)[CH3:8]参加物
4
実験手順
3-Amino-N,N-dimethyl-5-trifluoromethyl-benzamide (2.0 g; 8.6 mmol) dissolved in THF (20 ml) is reduced with a 1 M solution of BH3.THF (26 ml) as described in Stage 134.1, yielding the title compound: MS: [M+1]+=219.
出典と根拠
- ORDレコード
- ord-ee3663fa87894d688ece044822727223
- 出典データセット
- uspto-grants-2010_01
- 特許番号
- US07652022B2
反応ノート
読み込み中…