3-Methoxypyridine-2-carboxylic acid → HCID 178492104、化合物
反応式
[CH3:1][O:2][C:3]1[C:4]([C:9]([OH:11])=O)=[N:5][CH:6]=[CH:7][CH:8]=1.[NH2:12][C:13]1[NH:17][N:16]=[N:15][N:14]=1>S(Cl)(Cl)=O>[NH:14]1[C:13]([NH:12][C:9]([C:4]2[C:3]([O:2][CH3:1])=[CH:8][CH:7]=[CH:6][N:5]=2)=[O:11])=[N:17][N:16]=[N:15]1参加物
4
実験手順
1.45 g of 3-methoxy-2-pyridinecarboxylic acid, 30 ml of thionyl chloride and 0.95 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from a mixture of dimethylformamide and water, whereby 0.18 g of N-(5-tetrazolyl)-3-methoxy-2-pyridinecarboxamide is obtained.
後処理
- customThe crude product thus obtained
- customis recrystallized from a mixture of dimethylformamide and water
出典と根拠
- ORDレコード
- ord-25899d86f68e4a6396d8757f51e06fec
- 出典データセット
- uspto-grants-1983_09
- 特許番号
- US04404214
反応ノート
読み込み中…