化工社化工社 化学情報印刷レポート · 研究参考用
6-Butoxypicolinic acid → HCID 178450155、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Butoxypicolinic acid | HCID 13209546 | — |
| 反応物 | HCID 178509299 | HCID 178509299 | — |
| 溶媒 | Thionyl Chloride | HCID 24386 | — |
| 生成物 | HCID 178450155 | HCID 178450155 | 61% |
反応手順
0.94 g of 6-n-butoxy-2-pyridinecarboxylic acid, 10 ml of thionyl chloride and 0.48 g of 5-aminotetrazole are treated in the same manner as described in Example 1. The crude product thus obtained is recrystallized from a mixture of dimethylformamide, water and ethanol, whereby 0.77 g of N-(5-tetrazolyl)-6-n-butoxy-2-pyridinecarboxamide is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04404214 |
| 出典データセット | uspto-grants-1983_09 |
| ORD ID | ord-68b50df34b4e498683547342c1c3dcfd |
| 出典メモ | uspto-grants-1983_09 |