反応式
[C:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9]Br)(=[O:3])[CH3:2].[P:11]([O:18]CC)([O:15][CH2:16][CH3:17])[O:12][CH2:13][CH3:14]>>[C:1]([O:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][P:11]([O:15][CH2:16][CH3:17])([O:12][CH2:13][CH3:14])=[O:18])(=[O:3])[CH3:2]参加物
3
実験手順
100.34 g (0.48 mol) of 5-bromopentyl acetate were heated at 150° C. for 8 hours with 79.8 g (0.048 mol) of triethyl phosphite while stirring and passing in nitrogen. The mixture was then fractionally distilled under reduced pressure.
後処理
- distillationThe mixture was then fractionally distilled under reduced pressure
出典と根拠
- ORDレコード
- ord-37e8c73db5a4451484b91a4dd3cc9bb3
- 出典データセット
- uspto-grants-1998_03
- 特許番号
- US05728686
関連ノート
読み込み中…