HCID 68427706、化合物 → HCID 68427809、化合物
反応式
[CH3:1][N:2]1[CH2:6][CH2:5][CH:4]2[N:7]([C:10]3[CH:15]=[CH:14][C:13]([N+:16]([O-])=O)=[CH:12][CH:11]=3)[CH2:8][CH2:9][CH:3]12>CO.[Pd]>[CH3:1][N:2]1[CH:3]2[CH:4]([N:7]([C:10]3[CH:15]=[CH:14][C:13]([NH2:16])=[CH:12][CH:11]=3)[CH2:8][CH2:9]2)[CH2:5][CH2:6]1参加物
4
実験手順
1-Methyl-4-(4-nitrophenyl)octahydropyrrolo[3,2-b]pyrrole was hydrogenated by method B using methanol as solvent and palladium on carbon (5%) as catalyst. The product with the molecular weight of 217.32 (C13H19N3); MS (ESI): 218 (M+H+) was obtained in this way.
後処理
- customMS (ESI): 218 (M+H+) was obtained in this way
出典と根拠
- ORDレコード
- ord-d272a23473e74b58ac76c61fefb66c3e
- 出典データセット
- uspto-grants-2013_11
- 特許番号
- US08586609B2
反応ノート
読み込み中…