化工社化工社 化学情報印刷レポート · 研究参考用
Succinic Acid → 1-Cyclooctylmethylimidazole hydrogen succinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Succinic Acid | HCID 1110 | — |
| 反応物 | 1-Cyclooctylmethylimidazole | HCID 20550238 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 1-Cyclooctylmethylimidazole hydrogen succinate | HCID 20550250 | 44.7% |
反応手順
A solution of succinic acid (0.23 g) in ethanol (~5 ml) was added to a solution of 1-cyclooctylmethylimidazole (0.38 g) in ethanol (5 ml). Evaporation of the solution afforded a white solid. Recrystallisation of the solid from ethyl acetate afforded 1-cyclooctylmethylimidazole hydrogen succinate (0.27 g) as colourless plates, m.p. 86° to 87° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04317830 |
| 出典データセット | uspto-grants-1982_03 |
| ORD ID | ord-f3c8a4fd58044f61b41eedb23a9e3b99 |
| 出典メモ | uspto-grants-1982_03 |