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Hydrochloric Acid → 2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 3-(4-fluorophenoxy)-benzyl ester

HRID 2058669
ノート
印刷プレビュー

反応式

HRID 2058669 の反応式
[F:1][C:2]1[CH:16]=[CH:15][C:5]([O:6][C:7]2[CH:8]=[C:9]([CH:12]=[CH:13][CH:14]=2)[CH2:10][OH:11])=[CH:4][CH:3]=1.[CH3:17][C:18]1([CH3:26])[C:20]([CH3:22])([CH3:21])[CH:19]1[C:23](Cl)=[O:24].N1C=CC=CC=1.Cl>C1(C)C=CC=CC=1.O>[F:1][C:2]1[CH:16]=[CH:15][C:5]([O:6][C:7]2[CH:8]=[C:9]([CH:12]=[CH:13][CH:14]=2)[CH2:10][O:11][C:23]([CH:19]2[C:20]([CH3:22])([CH3:21])[C:18]2([CH3:26])[CH3:17])=[O:24])=[CH:4][CH:3]=1
参加物実験手順後処理出典と根拠反応ノート

参加物

7

反応物 4

HCID 313Hydrochloric AcidHCID 1049PyridineHCID 10584901[3-(4-Fluorophenoxy)phenyl]methanolHCID 110410022,2,3,3-Tetramethylcyclopropane-1-carbonyl chloride

生成物 1

HCID 128843492,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 3-(4-fluorophenoxy)-benzyl ester収率 81.9%

試薬・触媒・溶媒 2

HCID 962
Water
溶媒
HCID 1140Toluene溶媒2 回

実験手順

5.05 g (0.0232 mol) of 3-(4-fluoro-phenoxy)-benzyl alcohol and 3.72 g (0.0232 mol) of 2,2,3,3-tetramethylcyclopropanecarboxylic acid chloride were dissolved in 100 ml of anhydrous toluene, and 2.3 g of pyridine, dissolved in 50 ml of anhydrous toluene, were added dropwise at 20°-25° C., while stirring. The reaction mixture was then stirred for a further 3 hours at 25° C. It was poured into 150 ml of water, to which 10 ml of concentrated hydrochloric acid had been added, and the organic phase was separated off and washed again with 100 ml of water. The toluene phase was then dried over sodium sulphate and the solvent was distilled off under a waterpump vacuum. Last residues of solvent were removed by brief incipient distillation at a bath temperature of 60° C./1 mm Hg. 6.5 g (81.9% of theory) of 2,2,3,3-tetramethyl-cyclopropanecarboxylic acid 3-(4-fluorophenoxy)-benzyl ester were obtained as a yellow oil with a refractive index nD20 of 1.5348.

後処理

  1. additionwere added dropwise at 20°-25° C.
  2. stirringThe reaction mixture was then stirred for a further 3 hours at 25° C
  3. additionhad been added
  4. customthe organic phase was separated off
  5. washwashed again with 100 ml of water
  6. dry with materialThe toluene phase was then dried over sodium sulphate
  7. distillationthe solvent was distilled off under a waterpump vacuum
  8. customLast residues of solvent were removed by brief incipient distillation at a bath temperature of 60° C./1 mm Hg

出典と根拠

ORDレコード
ord-a1ad5e5b8c524e6893b300051c584a3c
出典データセット
uspto-grants-1982_03
DOI
10.6084/m9.figshare.5104873.v1
特許番号
US04318922

反応ノート

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