4-Methoxybenzaldehyde → ethyl (E)-3-(4-methoxyphenyl)-2-methylprop-2-enoate
反応式
COc1ccc(C=O)cc1.CCOC(=O)C(C)C(=O)O>C1COCCN1.CN(C)c1ccncc1.C1CCOC1>CCOC(=O)/C(C)=C/c1ccc(OC)cc1参加物
6
反応条件
- 温度
- 25 °C
後処理
- temperatureThe product mixture was cooled to 25 °C.
- filtrationFiltered through a pad of celite · Organic 相を保持
- wash"The celite was washed with ethyl acetate (3 x 1 mL)."
- concentrationThe filtrate was concentrated under reduced pressure
- additionA 0.07 M stock solution of the internal standard ethylene carbonate (0.70 mL in CDCl3) was added.
出典と根拠
- ORDレコード
- ord-4aac4172a31649d2baa61a35b64e3070
- 出典データセット
- Transfer learning optimization of 26 decarboxylative olefination reactions
反応ノート
読み込み中…