Piperonal → Ilepcimide
反応式
O=Cc1ccc2c(c1)OCO2.O=C(O)CC(=O)N1CCCCC1>C1COCCN1.CN(C)c1ccncc1.C1CCOC1>O=C(/C=C/c1ccc2c(c1)OCO2)N1CCCCC1参加物
6
反応条件
- 温度
- 25 °C
後処理
- temperatureThe product mixture was cooled to 25 °C.
- filtrationFiltered through a pad of celite · Organic 相を保持
- wash"The celite was washed with ethyl acetate (3 x 1 mL)."
- concentrationThe filtrate was concentrated under reduced pressure
- additionA 0.07 M stock solution of the internal standard ethylene carbonate (0.70 mL in CDCl3) was added.
出典と根拠
- ORDレコード
- ord-cf7aa6ded56c47588d809974808d1c23
- 出典データセット
- Transfer learning optimization of 26 decarboxylative olefination reactions
反応ノート
読み込み中…