(4-Chlorophenoxy)acetic acid → 2-[(4-Chlorophenyl)methoxy]acetic acid

HRID 2069327ノート

反応式

HRID 2069327 の反応式
ClC1C=CC([O:6][CH2:7][C:8]([OH:10])=[O:9])=CC=1.[Cl:13][C:14]1[CH:21]=[CH:20][C:17]([CH2:18]Br)=[CH:16][CH:15]=1>>[Cl:13][C:14]1[CH:21]=[CH:20][C:17]([CH2:18][O:6][CH2:7][C:8]([OH:10])=[O:9])=[CH:16][CH:15]=1

参加物

3

反応物 2

HCID 26229(4-Chlorophenoxy)acetic acidHCID 693291-(Bromomethyl)-4-chlorobenzene

生成物 1

HCID 3520062-[(4-Chlorophenyl)methoxy]acetic acid

実験手順

(4-Chlorobenzyloxy)acetic acid was prepared in analogy to (4-chlorophenoxy)-acetic acid using 4-chlorobenzyl bromide as precursor. The product with the molecular weight of 200.62 (C9H9ClO3) was obtained in this way; MS (ESI): 222.95 (M+Na—H).

後処理

  1. customThe product with the molecular weight of 200.62 (C9H9ClO3) was obtained in this way

出典と根拠

ORDレコード
ord-b51aafa3feb948fb8ed84debab544d9a
出典データセット
uspto-grants-2012_10
特許番号
US08299104B2

反応ノート

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