Pyridine → 2,2,3,4,4,4-Hexafluorobutyl 11-pyridylundecylate bromide

HRID 2071920

反応式

HRID 2071920 の反応式
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O:14][CH2:15][C:16]([F:24])([F:23])[CH:17]([F:22])[C:18]([F:21])([F:20])[F:19])=[O:13].[N:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>>[Br-:1].[N:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([O:14][CH2:15][C:16]([F:24])([F:23])[CH:17]([F:22])[C:18]([F:21])([F:20])[F:19])=[O:13]

参加物

3

反応物 2

HCID 1049PyridineHCID 214099962,2,3,4,4,4-Hexafluorobutyl 11-bromoundecylate

生成物 1

HCID 214099972,2,3,4,4,4-Hexafluorobutyl 11-pyridylundecylate bromide

実験手順

The process of claim 2 comprising (a) reacting at reflux about 1 mole of 2,2,3,4,4,4-hexafluorobutanol and about 1 mole of 11-bromoundecanoic acid to obtain 2,2,3,4,4,4-hexafluorobutyl 11-bromoundecylate and then (b) reacting about 1 mole of 2,2,3,4,4,4-hexafluorobutyl 11-bromoundecylate with about 1 mole pyridine to obtain 2,2,3,4,4,4-hexafluorobutyl 11-pyridylundecylate bromide.

出典と根拠

ORDレコード
ord-601a59fe58c940c982dff2ba5bb38c3b
出典データセット
uspto-grants-1977_09
特許番号
US04049668

関連ノート

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