化工社化工社 化学情報印刷レポート · 研究参考用
Suberic acid → Oxonane-2,9-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Suberic acid | HCID 10457 | — |
| 溶媒 | Acetic Anhydride | HCID 7918 | — |
| 生成物 | Oxonane-2,9-dione | HCID 9543534 | 50.4% |
反応手順
A solution of suberic acid (5.0 g, 28.7 mmol) in acetic anhydride (10 mL) was heated at reflux for 1 h. After cooling to RT, the solvent was removed in vacuo. The pale yellow residue was recrystallized from acetonitrile. After filtration and drying to the vacuum pump, the oxonane-2,9-dione was obtained as a white solid (2.26 g, 50.4% yield).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07923579B2 |
| 出典データセット | uspto-grants-2011_04 |
| ORD ID | ord-de2bb5712e94419a90ec52684ee6e963 |
| 出典メモ | uspto-grants-2011_04 |