反応式
[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S:11]([NH:14][C:15]2[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][C:16]=2[C:22]([C:24]2[CH:29]=[CH:28][N:27]=[CH:26][CH:25]=2)=[O:23])(=[O:13])=[O:12])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[BH4-].[Na+]>>[C:1]([C:5]1[CH:10]=[CH:9][C:8]([S:11]([NH:14][C:15]2[CH:20]=[CH:19][C:18]([Cl:21])=[CH:17][C:16]=2[CH:22]([OH:23])[C:24]2[CH:29]=[CH:28][N:27]=[CH:26][CH:25]=2)(=[O:13])=[O:12])=[CH:7][CH:6]=1)([CH3:4])([CH3:2])[CH3:3]参加物
3
実験手順
The title compound was prepared by the reduction of 4-tert-Butyl-N-[4-chloro-2-(pyridine-4-carbonyl)-phenyl]-benzenesulfonamide with NaBH4 according to the procedure described in the preceding example. MS: (M+H)=431.
出典と根拠
- ORDレコード
- ord-ef95b760d6db4cdebf0882c3a23ede56
- 出典データセット
- uspto-grants-2011_04
- 特許番号
- US07932252B2
関連ノート
読み込み中…