Ethanolamine → HCID 20357536、化合物

HRID 2083727ノート

反応式

HRID 2083727 の反応式
[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][C:9]=2[N:11]=[C:12]=S)[CH:4]=[N:3]1.[CH2:14]([CH2:16][NH2:17])[OH:15]>CCOCC>[CH3:1][N:2]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][C:9]=2[NH:11][C:12]2[O:15][CH2:14][CH2:16][N:17]=2)[CH:4]=[N:3]1

参加物

4

反応物 2

HCID 700EthanolamineHCID 203575387-Isothiocyanato-1-methyl-1H-indazole

生成物 1

HCID 20357536HCID 20357536、化合物

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

実験手順

The starting material is prepared as follows: 3 g of 1-methyl-7-isothiocyanato-indazole is added to a stirred mixture of 2 ml of ethanolamine and 100 ml of ether, thus forming a white precipitate. After 2 hours the precipitate is filtered off and washed with ether to yield the starting material; M.Pt. 207° - 209°.

後処理

  1. customThe starting material is prepared
  2. customthus forming a white precipitate
  3. filtrationAfter 2 hours the precipitate is filtered off
  4. washwashed with ether
  5. customto yield the starting material

出典と根拠

ORDレコード
ord-5e502b75df0b4d0aaee63fbe985baa8a
出典データセット
uspto-grants-1978_04
特許番号
US04086353

反応ノート

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